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Injection technique, solvent type, and vial pressure differentials all play measurable roles, yet most standard operating procedures address only the solvent volume and never mention the mechanical stressors that cause the majority of early failures

10.1016/s0968-0896(00)00294-7 76 LukaszukA.DemaegdtH.FeytensD.VanderheydenP.VauquelinG.TourwD